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Regions of hypoxia occur in most solid tumours and are known to significantly impact therapy response and patient prognosis. Ag5 is a recently reported silver molecular cluster which inhibits both glutathione and thioredoxin signalling therefore limiting cellular antioxidant capacity. Ag5 treatment significantly reduces cell viability in a range of cancer cell lines with little to no impact on non-transformed cells. Characterisation of redox homeostasis in hypoxia demonstrated an increase in reactive oxygen species and glutathione albeit with different kinetics. Significant Ag5-mediated loss of viability was observed in a range of hypoxic conditions which mimic the tumour microenvironment however, this effect was reduced compared to normoxic conditions. Reduced sensitivity to Ag5 in hypoxia was attributed to HIF-1 mediated signalling to reduce PDH via PDK1/3 activity and changes in mitochondrial oxygen availability. Importantly, the addition of Ag5 significantly increased radiation-induced cell death in hypoxic conditions associated with radioresistance. Together, these data demonstrate Ag5 is a potent and cancer specific agent which could be used effectively in combination with radiotherapy.

Original publication

DOI

10.1016/j.redox.2024.103326

Type

Journal

Redox Biol

Publication Date

10/2024

Volume

76

Keywords

Ag5, HIF-1, Hypoxia, Radiation, Redox, Humans, Signal Transduction, Oxygen, Reactive Oxygen Species, Cell Survival, Cell Line, Tumor, Glutathione, Hypoxia-Inducible Factor 1, alpha Subunit, Mitochondria, Pyruvate Dehydrogenase Acetyl-Transferring Kinase, Cell Hypoxia, Protein Serine-Threonine Kinases, Neoplasms, Oxidation-Reduction, Hypoxia-Inducible Factor 1, Silver, Antineoplastic Agents